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Journal of Vacuum Science and Technology B: Microelectronics and Nanometer StructuresVolume 26, Issue 5, 2008, Pages 1761-1764

Fabrication of gold tips suitable for tip-enhanced Raman spectroscopy(Article)

  • aNational Physical Laboratory, Teddington TW11 0LW, United Kingdom
  • bH. H. Wills Physics Laboratory, University of Bristol, Tyndall Avenue, Bristol BS8 1TL, United Kingdom

Abstract

The authors report on a simple method of fabricating gold tips, suitable for use in a shear-force mode atomic force microscope for tip-enhanced Raman spectroscopy (TERS). The proposed electrochemical method is highly optimized and offers five advantages: produces a low-aspect ratio tip that can withstand the lateral force at the end of the tip during scanning, produces a sharp tip end to generate good Raman enhancements for TERS, a self-terminating process that makes the etching process easy, use of inexpensive electronic systems so that it can be adopted by any laboratory, and less time consuming (takes less than 20 s to fabricate a single tip). This article demonstrates TERS imaging using such tips. © 2008 American Vacuum Society.

Indexed keywords

Engineering controlled terms:Architectural acousticsAspect ratioFabricationRaman scatteringRaman spectroscopySpectrum analysis
Engineering uncontrolled terms:Atomic Force MicroscopeElectro-chemical methodElectronic systemsEtching processesLateral forcesSharp tipSimple methodsTime consumingTip-enhanced Raman Spectroscopy
Engineering main heading:Atomic spectroscopy

Funding details

Funding numberFunding sponsorAcronymFunding opportunities
National Physical LaboratoryNPL
  • 1

    The authors gratefully acknowledge the help of Gareth Hind for voltammogram measurements. This work at the National Physical Laboratory was funded by the Strategic Research Committee.

  • ISSN: 10711023
  • CODEN: JVTBD
  • Source Type: Journal
  • Original language: English
  • DOI: 10.1116/1.2981078
  • Document Type: Article

  Roy, D.; National Physical Laboratory, United Kingdom;
© Copyright 2008 Elsevier B.V., All rights reserved.

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