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MaterialsVolume 16, Issue 13, July 2023, Article number 4760

Processing of Niobium-Alloyed High-Carbon Tool Steel via Additive Manufacturing and Modern Powder Metallurgy(Article)(Open Access)

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  • aDepartment of Metals and Corrosion Engineering, University of Chemistry and Technology, Prague, Technická 5, Prague, 166 28, Czech Republic
  • bComtes FHT a.s, Průmyslová 995, Dobrany, 334 41, Czech Republic
  • cDepartment for Production Engineering, Faculty of Technical Science, University of Novi Sad, Trg Dositeja Obradovica 6, Novi Sad, 21000, Serbia

Abstract

Niobium is recently considered one of the potential alloying elements for tool steels due to the formation of hard and stable carbides of MC type. Its use is limited by the fact that these carbides tend to coarsen during conventional melting metallurgy processing. This work explores the potential of additive manufacturing for processing Nb-alloyed tool steel with a high content of carbon. Directed energy deposition was used as the processing method. It was found that this method allowed us to obtain a microstructure very similar to that obtained after the use of consolidation via spark plasma sintering when subsequent heat treatment by soft annealing, austenitizing, oil quenching and triple tempering for secondary hardness was applied. Moreover, the soft annealing process could be skipped without affecting the structure and properties when machining would not be required. The hardness of the steel was even higher after additive manufacturing was used (approx. 800–830 HV 30) than after spark plasma sintering (approx. 720–750 HV 30). The wear resistance of the materials processed by both routes was almost comparable, reaching 5–7 × 10−6 mm3N−1m−1 depending on the heat treatment. © 2023 by the authors.

Author keywords

carbidesheat treatmentniobiumtool steel

Indexed keywords

Engineering controlled terms:3D printingAdditivesAlloying elementsCarbidesHardnessHeat resistanceNiobium alloysPowder metallurgySpark plasma sinteringWear resistance
Engineering uncontrolled termsAustenitizingDirected energyEnergy depositionsHigh carbon tool steelHigh-contentOil quenchingProcessing methodSoft annealingSpark-plasma-sinteringTriple tempering
Engineering main heading:Tool steel

Funding details

Funding sponsor Funding number Acronym
European Regional Development FundA2_FCHT_2023_015,CZ02.1.01/0.0/0.0/16_019/0000836ERDF
  • 1

    The study was supported by ERDF Research of advanced steels with unique properties, grant no. CZ02.1.01/0.0/0.0/16_019/0000836. This work was also supported by a grant for Specific university research, grant no. A2_FCHT_2023_015.

  • ISSN: 19961944
  • Source Type: Journal
  • Original language: English
  • DOI: 10.3390/ma16134760
  • Document Type: Article
  • Publisher: Multidisciplinary Digital Publishing Institute (MDPI)

  Borkovcová, K.; Department of Metals and Corrosion Engineering, University of Chemistry and Technology, Prague, Technická 5, Prague, Czech Republic;
© Copyright 2023 Elsevier B.V., All rights reserved.

Cited by 1 document

Hentschel, O. , Kohlstruck, J. , Vetter, J.
Experimental Investigations in the Processing of AISI H11 Powder Blends Enriched with Tungsten Carbide Nanoparticles for the Additive Manufacturing of Tailored Hot Working Tools in the Directed Energy Deposition (DED-LB/M)—Impact of Tungsten Carbide Nanoparticles on Microstructural and Mechanical Characteristics
(2024) Metals
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